(2S)-2-[[2-(3,5-difluorophenyl)acetyl]amino]propanoic acid → HCID 9953534, compound

Participants

Reaction Steps

Following General Procedure A and using N-(3,5-difluorophenylacetyl)-L-alanine (from Example B2 above) and Nε,Nε-dimethyl-L-lysine methyl ester hydrochloride (Bachem), the title compound was prepared as a solid (mp=123-126° C.). The reaction was monitored by tlc (Rf=0.22 in 10% MeOH/DCM+1% TEA) and the product was purified by silica gel column chromatography.

Provenance & Evidence