HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 22894828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 22895005 | HCID 22895005 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 22894828 | HCID 22894828 | — |
Reaction Steps
Following General Procedure C and using N-[N-(3,5-difluorophenylacetyl)-L-alaninyl]-L-alanine (from Example D7 above) and pyrrolidine (Aldrich), the title compound was prepared as a solid. The reaction was monitored by tlc (Rf=0.15 in 95:5 CHCl3/MeOH) and the product was purified by silica gel chromatography using CHCl3/MeOH as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06191166B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-cd8b2865f9884a2caa89596069d5f333 |
| Source note | uspto-grants-2001_02 |