HuagongsheHuagongshe Chemistry Print Report · For research reference only
methyl L-prolinate hydrochloride → N-(N-(Phenylacetyl)-L-alaninyl]-L-proline Methyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | methyl L-prolinate hydrochloride | HCID 2733200 | — |
| Reactant | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| Product | N-(N-(Phenylacetyl)-L-alaninyl]-L-proline Methyl Ester | HCID 22895052 | — |
Reaction Steps
Following General Procedure A and using N-(phenylacetyl)-L-alanine (from Example B1 above) and L-proline methyl ester hydrochloride (Bachem), the title compound was prepared as an oil. The reaction was monitored by tlc (Rf=0.12 in 50% EtOAc/hexanes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06191166B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-47d2b74abf3a4f92be9e72b7b975bd3b |
| Source note | uspto-grants-2001_02 |