HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl valinate hydrochloride → HCID 22895053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl valinate hydrochloride | HCID 111190 | — |
| Reactant | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| Product | HCID 22895053 | HCID 22895053 | — |
Reaction Steps
Following General Procedure A and using N-(phenylacetyl)-L-alanine (fromo Example B1 above) and L-valine methyl ester hydrochloride (Aldrich), the title compound was prepared as a solid (mp=112-115° C.). The reaction was monitored by tlc (Rf=0.33 in 50% EtOAc/hexanes) and the product was not purified.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06191166B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-293bbc5a8fbe4d579b27a87ae685970c |
| Source note | uspto-grants-2001_02 |