Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 636303Generated: November 1, 2026

1,4-Dioxane hydrochloride → HCID 54539135, compound

https://huagongshe.com/reaction/636303

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,4-Dioxane hydrochlorideHCID 20443148—
ReactantHCID 21257558HCID 21257558—
ProductHCID 54539135HCID 54539135—

Reaction Steps

A solution of ethyl 2-(N-Boc-N-ethylamino)-6-pyridylacetate (1.5 g, 4.87 mmol) and 4M HCl/dioxane (5 mL, 20 mol) was stirred at RT overnight, then was concentrated. Reconcentration from toluene gave the title compound as white solid: MS (ES) m/e 209 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06191304B1
Source datasetuspto-grants-2001_02
ORD IDord-6e4cfb451cba429b8fe195d1437e8634
Source noteuspto-grants-2001_02