HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 636342Generated: October 29, 2026
Allyl bromide → N-allyl-N-[4-(perfluorohexyl)phenyl]-2,4-dinitrobenzenamine
https://huagongshe.com/reaction/636342
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 22735010 | HCID 22735010 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | N-allyl-N-[4-(perfluorohexyl)phenyl]-2,4-dinitrobenzenamine | HCID 22734998 | — |
Reaction Steps
A mixture of N-[4-(perfluorohexyl)phenyl]-2,4-dinitrobenzenamine (3.6 g, 6.2 mmol), NMP (40 mL), potassium carbonate (3.0 g) and allyl bromide (0.65 mL) was stirred at 75° C. for 4 hr. The mixture was extracted in the normal fashion, and the product recrystallized to give N-allyl- N-[4-(perfluorohexyl)phenyl]-2,4-dinitrobenzenamine (2.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06194039B1 |
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| Source dataset | uspto-grants-2001_02 |
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| ORD ID | ord-52649c67c77e4c60adb2a9d698bdea5b |
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| Source note | uspto-grants-2001_02 |
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