HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 21254969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 7-Chloro-3-(4-chloro-benzenesulphonyl)-5-methyl-2-methylsulphanyl-pyrazolo[1,5-a]pyrimidine | HCID 21254986 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21254969 | HCID 21254969 | — |
Reaction Steps
In an analogous manner to that described in Example 5, from 7-chloro-3-(4-chloro-benzenesulphonyl)-5-methyl-2-methylsulphanyl-pyrazolo[1,5-a]pyrimidine and dimethyl-amine in EtOH there was obtained [3-(4-chloro-benzenesulphonyl)-5-methyl-2-methylsulphanyl-pyrazolo[1,5-a]pyrimidin-7-yl]-dimethyl-amine as colorless crystals, m.p. 221-223°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06194410B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-96f129ed65e14d3aa4e889ef5232ddbb |
| Source note | uspto-grants-2001_02 |