HRID636489
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of 2,6-dimethyl-3-nitrobenzyl acetate (26.9 g) in methanol (266 ml) was added 1N sodium hydroxide solution (133 ml) at ambient temperature, and the mixture was stirred for 30 minutes. To the reaction mixture was added water, and the resulting precipitates were collected by filtration to give 2,6-dimethyl-3-nitrobenzyl alcohol (18.0 g) as pale yellow crystals.
WORKUP
后处理
- customthe resulting precipitates
- filtrationwere collected by filtration