(4-Quinolyl)methylene-1,2-dimethoxyfluorene → 9-(Phenylmethylene)-1,2-dimethoxyfluorene

HRID 636651Notes

Reaction equation

HRID 636651 reaction equation
N1C2C(=CC=CC=2)C([CH:11]=[C:12]2[CH:24]=[C:23]3[C:15](=[CH:16][C:17]4[C:22]3=[CH:21][CH:20]=[CH:19][CH:18]=4)[C:14]([O:25][CH3:26])=[C:13]2[O:27][CH3:28])=CC=1>CC(C)=O.C1CCCCC1>[C:12]1([CH:24]=[C:23]2[C:15]3[C:14]([O:25][CH3:26])=[C:13]([O:27][CH3:28])[CH:12]=[CH:11][C:16]=3[C:17]3[C:22]2=[CH:21][CH:20]=[CH:19][CH:18]=3)[CH:24]=[CH:23][CH:15]=[CH:14][CH:13]=1

Participants

3

Reactant 1

HCID 86756455(4-Quinolyl)methylene-1,2-dimethoxyfluorene

Product 1

HCID 536881979-(Phenylmethylene)-1,2-dimethoxyfluorene

Reagents, catalysts & solvents 1

HCID 21916603Acetone cyclohexaneSolvent

Procedure

9-((4-Quinolyl)methylene-1,2-dimethoxyfluorene; m.p. 210° C. (acetone/cyclohexane). Anal. Calcd. for C25H19NO2: C, 82.17; H, 5.24; N, 3.83. Found: C, 82.23; H, 5.00; N, 3.88.

Sources & evidence

ORD record
ord-ba4b668849694e2887f8bff4993a2d6c
Source dataset
uspto-grants-2001_02
Patent number
US06194439B1

Reaction notes

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