1,4-Butanedisulfonyl dichloride → 1,4-Benzenedithiol 1,4-butanedisulfonylchloride

Participants

Reaction Steps

Next, the 1,4-butanedisulfonyl chloride vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 15 minutes. Consequently, 1,4-butanedisulfonyl chloride condensed on the surface of the base particles. A polymerization reaction, using as a catalyst triethylamine contained in the base particles, took place between 1,4-butanedisulfonyl chloride condensed on the surface of the base particles and 1,4-benzenedithiol contained therein, forming a film of 1,4-benzenedithiol-1,4-butanedisulfonylchloride co-polymer on the surface of the base particles.

Provenance & Evidence