1,3-Propanediamine → HCID 21255761, compound
Reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][NH2:5].[CH2:6]([S:13]([Cl:16])(=[O:15])=[O:14])[CH2:7][CH2:8][S:9]([Cl:12])(=[O:11])=[O:10]>>[CH2:8]([S:9]([Cl:12])(=[O:10])=[O:11])[CH2:7][CH2:6][S:13]([Cl:16])(=[O:15])=[O:14].[NH2:1][CH2:2][CH2:3][CH2:4][NH2:5]Participants
3
Procedure
Next, the 1,3-diaminopropane vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 2 minutes. Consequently, 1,3-diaminopropane condensed on the surface of the base particles. A polymerization reaction took place between 1,3-diaminopropane condensed on the surface of the base particles and 1,3-propanedisulfonyl chloride making up the base particles, forming a film of 1,3-propanedisulfonylchloride-1,3-diaminopropane co-polymer on the surface of the base particles.
Workup
- customA polymerization reaction
Sources & evidence
- ORD record
- ord-12cb48748d34429f8cc12b76fa737459
- Source dataset
- uspto-grants-2001_02
- Patent number
- US06194487B1
Reaction notes
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