1,4-Diaminocyclohexane → HCID 86756469, compound

HRID 636781Notes

Reaction equation

HRID 636781 reaction equation
[NH2:1][CH:2]1[CH2:7][CH2:6][CH:5]([NH2:8])[CH2:4][CH2:3]1.[C:9]1([CH3:25])[CH:14]=[C:13]([CH3:15])[C:12]([S:16]([Cl:19])(=[O:18])=[O:17])=[C:11]([CH3:20])[C:10]=1[S:21]([Cl:24])(=[O:23])=[O:22]>>[C:9]1([CH3:25])[CH:14]=[C:13]([CH3:15])[C:12]([S:16]([Cl:19])(=[O:18])=[O:17])=[C:11]([CH3:20])[C:10]=1[S:21]([Cl:24])(=[O:22])=[O:23].[NH2:1][CH:2]1[CH2:7][CH2:6][CH:5]([NH2:8])[CH2:4][CH2:3]1

Participants

3

Reactant 2

HCID 183741,4-Diaminocyclohexane2×HCID 36200812,4-Mesitylenedisulfonyl Dichloride

Product 1

HCID 86756469HCID 86756469, compound

Procedure

Next, the 1,4-diaminocyclohexane vapor in the condensing chamber 2 was adiabatically expanded, and the introduced modified particles (27) were exposed thereto for 2 minutes. Consequently, a further polymerization reaction between 2,4-mesitylenedisulfonyl chloride and 1,4-diaminocyclohexane took place on the surface of the modified particles (27), forming a film of 2,4-mesitylenedisulfonyl chloride-1,4-diaminocyclohexane co-polymer.

Sources & evidence

ORD record
ord-46c8bc10775249b9889da26db6c97570
Source dataset
uspto-grants-2001_02
Patent number
US06194487B1

Reaction notes

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