1,10-Decanediamine → 1,4-Butanedisulfonylchloride 1,10-diaminodecane

HRID 636783Notes

Reaction equation

HRID 636783 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][NH2:12].[CH2:13]([S:21]([Cl:24])(=[O:23])=[O:22])[CH2:14][CH2:15][CH2:16][S:17]([Cl:20])(=[O:19])=[O:18]>>[CH2:13]([S:21]([Cl:24])(=[O:22])=[O:23])[CH2:14][CH2:15][CH2:16][S:17]([Cl:20])(=[O:19])=[O:18].[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][NH2:12]

Participants

3

Reactant 2

HCID 13171,10-Decanediamine2×HCID 3153171,4-Butanedisulfonyl dichloride

Product 1

HCID 212557461,4-Butanedisulfonylchloride 1,10-diaminodecane

Procedure

Next, in the mixing section 22, the vapor atmosphere of 1,10-diaminodecane was cooled, and the introduced base particles were exposed thereto for 5 minutes. Consequently, a polymerization reaction took place on the surface of the base particles between 1,4-butanedisulfonyl chloride and 1,10-diaminodecane, forming a film of 1,4-butanedisulfonylchloride-1,10-diaminodecane co-polymer.

Workup

  1. customConsequently, a polymerization reaction

Sources & evidence

ORD record
ord-f4f154b64b48431aaeec80a1313fdcd8
Source dataset
uspto-grants-2001_02
Patent number
US06194487B1

Reaction notes

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