1,4-Butanedisulfonyl dichloride → HCID 86756470, compound
Reaction equation
[NH2:1][C:2]1[CH:7]=[C:6]([SH:8])[C:5]([NH2:9])=[CH:4][C:3]=1[SH:10].[CH2:11]([S:19]([Cl:22])(=[O:21])=[O:20])[CH2:12][CH2:13][CH2:14][S:15]([Cl:18])(=[O:17])=[O:16]>>[CH2:11]([S:19]([Cl:22])(=[O:20])=[O:21])[CH2:12][CH2:13][CH2:14][S:15]([Cl:18])(=[O:17])=[O:16].[NH2:1][C:2]1[CH:7]=[C:6]([SH:8])[C:5]([NH2:9])=[CH:4][C:3]=1[SH:10]Participants
3
Procedure
Next, the 2,5-diamino-1,4-benzenedithiol vapor in the condensing chamber 2 was adiabatically expanded, and the introduced modified particles (35) were exposed thereto for 18 minutes. Consequently, a further polymerization reaction between 1,4-butanedisulfonyl chloride and 2,5-diamino-1,4-benzenedithiol took place on the surface of the modified particles (35), forming a film of 1,4-butanedisulfonylchloride-2,5-diamino-1,4-benzenedithiol co-polymer.
Sources & evidence
- ORD record
- ord-b1994361f61e485ebefbc6593b353e4d
- Source dataset
- uspto-grants-2001_02
- Patent number
- US06194487B1
Reaction notes
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