HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → Ethylene glycol sebacoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Sebacoyl chloride | HCID 66072 | — |
| Product | Ethylene glycol sebacoyl chloride | HCID 86756477 | — |
Reaction Steps
The base particles, along with helium gas, were cooled and introduced through the particle intake 4 into the vapor atmosphere of sebacoyl chloride in the mixing section 22. Next, in the mixing section 22, the vapor of sebacoyl chloride was cooled, and the introduced base particles were exposed thereto for 2 minutes. Consequently, a polymerization reaction, using as a catalyst triethylamine contained in the base particles, took place on the surface of the base particles between sebacoyl chloride and ethylene glycol, forming a film of ethylene glycol-sebacoyl chloride co-polymer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06194487B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-e6a203c38b194da688c631e0db90473d |
| Source note | uspto-grants-2001_02 |