HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 637256Generated: October 25, 2026
3-(Chlorocarbonyl)phenyl acetate → N-(m-Acetoxybenzoyl)-S,S-dimethyl-sulphoximine
https://huagongshe.com/reaction/637256
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-(Chlorocarbonyl)phenyl acetate | HCID 12998558 | — |
| Reactant | Dimethyl sulphoximine potassium salt | HCID 86740516 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-(m-Acetoxybenzoyl)-S,S-dimethyl-sulphoximine | HCID 20256530 | — |
Reaction Steps
A solution of 99.3 g of m-acetoxybenzoyl chloride in 150 ml of absolute tetrahydrofuran is added dropwise at -35° C. during 20 minutes while stirring to the dimethyl sulphoximine potassium salt suspension and the mixture is then stirred at -35° C. for 30 minutes. N-(m-Acetoxybenzoyl)-S,S-dimethyl-sulphoximine is thus formed in suspension.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04556413 |
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| Source dataset | uspto-grants-1985_12 |
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| ORD ID | ord-7abe3c7ad9e0455ab3840a266774c0b4 |
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| Source note | uspto-grants-1985_12 |
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