HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 1-Methyl-4-phenoxymethyl-pyrrolidin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | p-Toluenesulfonate | HCID 85570 | — |
| Reactant | Potassium phenoxide | HCID 23670670 | — |
| Product | 1-Methyl-4-phenoxymethyl-pyrrolidin-2-one | HCID 13362252 | — |
Reaction Steps
A solution of the resulting tosylate (21.5 g; 0.075 mole) and of potassium phenoxide (10 g; 0.075 mole) in dimethylformamide (150 ml) is refluxed for 2 hrs.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04556674 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-d84526e153214697b4cb8e1d5ae29157 |
| Source note | uspto-grants-1985_12 |