HCID 20165166, compound → HCID 13362254, compound

HRID 637332Notes

Reaction equation

HRID 637332 reaction equation
[CH3:1][N:2]1[CH2:6][CH:5]([CH2:7][O:8]S(C2C=CC(C)=CC=2)(=O)=O)[CH2:4][C:3]1=[O:19].[CH2:20]([C:22]1[CH:28]=[CH:27][CH:26]=[CH:25][C:23]=1[O-])[CH3:21].[K+]>>[CH3:1][N:2]1[CH2:6][CH:5]([CH2:7][O:8][C:23]2[CH:25]=[CH:26][CH:27]=[CH:28][C:22]=2[CH2:20][CH3:21])[CH2:4][C:3]1=[O:19]

Participants

3

Reactant 2

HCID 20165166HCID 20165166, compoundHCID 23692206HCID 23692206, compound

Product 1

HCID 13362254HCID 13362254, compound

Procedure

The compound is prepared from 1-methyl-4-tosyloxymethyl-pyrrolidin-2-one described in Example 17, and potassium 2-ethyl-phenoxide, as described in Example 17. B.p. (0.3 mm Hg)=186° C.

Workup

  1. custom(0.3 mm Hg)=186° C.

Sources & evidence

ORD record
ord-e4fd50034f434c60bf8769bc760ac5cd
Source dataset
uspto-grants-1985_12
Patent number
US04556674

Reaction notes

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