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HRID637348

反应详情

EQUATION

反应方程式

HRID 637348 的结构方程式

REACTANTS

反应物

2
结构：O=C=NS(=O)(=O)Cl
HCID70918

Sulfuryl chloride isocyanate

CClNO3S

结构：O=C1Cc2cc3c(cc2N1)OCO3
HCID21282101

未命名化合物

PRODUCTS

生成物

1
结构：NC(=O)N1C(=O)Cc2cc3c(cc21)OCO3
HCID13647648

未命名化合物

PROCEDURE

实验过程

5,6-Methylenedioxy-2-oxindole-1-carboxamide was prepared by reaction of 5,6-methylenedioxy-2-oxindole with chlorosulfonyl isocyanate, followed by hydrolysis, using the procedure of Example 19. The product melted at 237°-238° C. (dec.) after recrystallization from acetic acid.

WORKUP

后处理

  1. customfollowed by hydrolysis
  2. customThe product melted at 237°-238° C. (dec.) after recrystallization from acetic acid