Sodium Hydroxide → HCID 89720726, compound

Participants

Reaction Steps

The title compound was prepared using a similar procedure as described in Example 1, Step 9, starting from (S)-2-[[1-(4-azidobutyl)cyclopentanecarbonyl]amino]-3-[4-(1,3,6-trimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)phenyl]propionic acid propyl ester (4.1 g, 7.42 mmol) and NaOH (35 mL, 35 mmol, 1M) which resulted in a white solid (3.75 g, 99%). ES(+)-HRMS m/e calcd. for C26H34N6O5 (M+H)+ 511.2664, obsd. 511.2664.

Provenance & Evidence