HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 20256928, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 20256926 | HCID 20256926 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20256928 | HCID 20256928 | 86.4% |
Reaction Steps
1,1 g (4 mmol) of 4-cyclopentyl-3-(p-methoxyphenyl)-3-hexanol was hydrogenated in an acidic medium for instance in acetic acid in the presence of some drops of methanesulfonic acid by using 10% Pd-C as a catalyst to yield 0.9 g (86%) of the oily product as a mixture of threo and erythro isomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04556677 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-b85b8f39201f40a18e4d58552a6be9f2 |
| Source note | uspto-grants-1985_12 |