HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium 2,4,6-trinitrobenzenesulfonate → HCID 86740531, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium 2,4,6-trinitrobenzenesulfonate | HCID 517400 | — |
| Reactant | HCID 10625993 | HCID 10625993 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86740531 | HCID 86740531 | 100.1% |
Reaction Steps
Dissolved in 5 ml of water was 5.28 g of 2-{4-(3-butoxy-2-hydroxypropoxy)phenylcarbamoyl}ethyldimethylsulfonium p-toluenesulfonate. To the solution was added a solution of 9 g of sodium picrylsulfonate in 10 ml of water. The crystals separating out were filtered off and recrystallized from ethanol, giving 6.50 g of 2-{4-(3-butoxy-2-hydroxypropoxy)phenylcarbamoyl}ethyldimethylsulfonium picrylsulfonate (Compound 15) in 93.5% yield, M.P. 106° to 108° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04556737 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-da02d0fab0e14dfa95cb139605ee9fcc |
| Source note | uspto-grants-1985_12 |