HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium 2,4,6-trinitrobenzenesulfonate → HCID 86740532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium 2,4,6-trinitrobenzenesulfonate | HCID 517400 | — |
| Reactant | HCID 20257053 | HCID 20257053 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86740532 | HCID 86740532 | 90.1% |
Reaction Steps
Dissolved in 2 ml of water was 4.45 g of 2-{2-(2,3-dihydroxypropoxy)phenoxy}ethyldimethylsulfonium p-toluenesulfonate. To the solution was added a solution of 6.30 g of sodium picrylsulfonate in 10 ml of water. The crystals formed were filtered off and recrystallized from ethanol, giving 5.10 g of 2-{2-(2,3-dihydroxypropoxy)phenoxy}ethyldimethylsulfonium picrylsulfonate in 90.1%, M.P. 124° to 125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04556737 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-4fb5a1722c4f4d3e92b3440509e6cff0 |
| Source note | uspto-grants-1985_12 |