Water → HCID 54328416, compound

Participants

Reaction Steps

3-Isobutenyl-1-octyn-3-ol (0.180 g; 10-3 mole) is kept at a temperature in the region of 40° C. and protected from light, in the presence of silver trifluoromethanesulphonate (0.257 g; 10-3 mole) in a mixture (10 cc) of tetrahydrofuran and water (3:1 by volume). After reacting for 7 hours the reaction mixture is treated under the conditions described in Example 1. 2-Methyl-1,4-undecadien-6-one (0.132 g) is obtained, having the following characteristics:

Provenance & Evidence