HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorophenol → HCID 13560229, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorophenol | HCID 7258 | — |
| Reactant | HCID 13560203 | HCID 13560203 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13560229 | HCID 13560229 | — |
Reaction Steps
6-Chloro-3-methylthio-2-pyridinecarbonitrile was mixed with 16.3 g of 3,4-dichlorophenol in the presence of 11.2 g of t-BuOK in 150 ml THF and 15 ml of DMSO. 13.4 g (54%) of the desired, 6-(3,4-dichlorophenoxy)-3-methylthio-2-pyridinecarbonitrile was recovered, m.p. 156°-158° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04558134 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-696e3e70c1a74939a3aa0c77c7d651b9 |
| Source note | uspto-grants-1985_12 |