HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorophenol → HCID 13560240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorophenol | HCID 7258 | — |
| Reactant | HCID 13560206 | HCID 13560206 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13560240 | HCID 13560240 | — |
Reaction Steps
6-Chloro-3-propylthio-2-pyridinecarbonitrile (12.8 g) was mixed with 10.6 g of 3,4-dichlorophenol in the presence of 7.3 g of t-BuOK in DMSO (10 ml) and THF (100 ml). The desired, 6-(3,4-dichlorophenoxy)-3-propylthio-2-pyridinecarbonitrile was recovered, m.p. 67°-69° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04558134 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-a4512637b126431e96f37e811d7d8555 |
| Source note | uspto-grants-1985_12 |