HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorophenol → HCID 13560241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorophenol | HCID 7258 | — |
| Reactant | HCID 13560207 | HCID 13560207 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13560241 | HCID 13560241 | — |
Reaction Steps
3-Chloro-6-propylthio-2-pyridinecarbonitrile (6.2 g) was mixed with 5.7 g of 3,4-dichlorophenol and 3.9 g of t-BuOK in 30 ml of DMSO and 30 ml THF. The desired, 3-(3,4-dichlorophenoxy)-6-propylthio-2-pyridinecarbonitrile was recovered, b.p. 203° C. (at 0.2 mm Hg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04558134 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-5173c0464f344c9f83df49005496a7a1 |
| Source note | uspto-grants-1985_12 |