HCID 20256271, compound → HCID 20256268, compound

HRID 637857Notes

Reaction equation

HRID 637857 reaction equation
[CH3:1][N:2]([CH3:24])[CH2:3][CH2:4][NH:5][C:6](=[O:23])[N:7]([CH:20]([CH3:22])[CH3:21])[CH2:8][CH2:9][O:10][C:11]1[CH:16]=[CH:15][C:14]([N+:17]([O-])=O)=[CH:13][CH:12]=1>[Pd]>[CH3:24][N:2]([CH3:1])[CH2:3][CH2:4][NH:5][C:6](=[O:23])[N:7]([CH:20]([CH3:21])[CH3:22])[CH2:8][CH2:9][O:10][C:11]1[CH:12]=[CH:13][C:14]([NH2:17])=[CH:15][CH:16]=1

Participants

3

Reactant 1

HCID 20256271HCID 20256271, compound

Product 1

HCID 20256268HCID 20256268, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

N'-[2-(dimethylamino)ethyl]-N-(1-methylethyl)-N-[2-(4-nitrophenoxy)ethyl]urea, free base in Example 62, is hydrogenated over palladium-on-charcoal catalyst to give the title compound.

Sources & evidence

ORD record
ord-b5fdb9030bbf470db8bce635a89b1e9c
Source dataset
uspto-grants-1985_12
Patent number
US04558155

Reaction notes

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