HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Bromide → DL-2-(4-chlorophenyl)propanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Bromide | HCID 6323 | — |
| Reactant | Methyl 4-chlorophenylacetate | HCID 104196 | — |
| Product | DL-2-(4-chlorophenyl)propanoic acid | HCID 102525 | — |
| Product | Methyl 2-(4-chlorophenyl)propanoate | HCID 12398854 | — |
Reaction Steps
The same reaction and the same treatment as in Example 1 were followed using methyl p-chlorophenylacetate and methyl bromide, producing methyl p-chloro(α-methyl)phenylacetate in a yield of 83% and p-chloro(α-methyl)phenylacetic acid in a yield of 5%. The spectral data of the ester were as follows.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04560447 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-874aa93ea73a4508a7e4b59f7852ae93 |
| Source note | uspto-grants-1985_12 |