HCID 13604098, compound → HCID 13604099, compound

HRID 638145Notes

Reaction equation

HRID 638145 reaction equation
[Cl:1][C:2]1[C:10]2[O:9][N:8]=[C:7]([CH2:11][CH:12]([CH3:14])[CH3:13])[C:6]=2[CH:5]=[C:4]2[CH2:15][CH:16]([C:18]([O:20]CC)=[O:19])[O:17][C:3]=12>C(OCC)(=O)C.CCCCCC>[Cl:1][C:2]1[C:10]2[O:9][N:8]=[C:7]([CH2:11][CH:12]([CH3:14])[CH3:13])[C:6]=2[CH:5]=[C:4]2[CH2:15][CH:16]([C:18]([OH:20])=[O:19])[O:17][C:3]=12

Participants

3

Reactant 1

HCID 13604098HCID 13604098, compound

Product 1

HCID 13604099HCID 13604099, compound

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

The above was obtained by analogous treatment of 7c and recrystallization from ethyl acetate/hexane; m.p. 181°-183° C. Anal. (C14H14ClNO4) C,H,N,Cl.

Sources & evidence

ORD record
ord-d21e7e4436c6491e8bf656698cfac4db
Source dataset
uspto-grants-1985_12
Patent number
US04560558

Reaction notes

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