Diethyl (ethoxymethylene)malonate → HCID 178469539, compound

Participants

Reaction Steps

From a mixture of 216 g of diethyl ethoxymethylenemalonate, 126.6 g of p-chloroaniline, and 800 ml of diphenyl heated first at 150°-160° for 15 min and then at 245° for 20 min there was obtained on cooling the above-named compound as a precipitate. This precipitate was collected, and washed with water and with hexane to give 245 g of crude damp solid, which was used directly in the hydrolysis reaction described below.

Provenance & Evidence