Ethyl benzoylacetate → HCID 178515553, compound

HRID 638295Notes

Reaction equation

[Cl:1][C:2]1[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][CH:3]=1.[C:9]([CH2:17][C:18](OCC)=[O:19])(=O)[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[Cl:1][C:2]1[CH:8]=[C:7]2[C:5](=[CH:4][CH:3]=1)[N:6]=[C:9]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[CH:17]=[C:18]2[OH:19]

Participants

Reactant 2

HCID 7170Ethyl benzoylacetate

HCID 78124-Chloroaniline

Product 1

HCID 178515553HCID 178515553, compound

Procedure

From 100 g of p-chloroaniline and 138.5 ml of ethyl benzoylacetate treated according to Example 4(a) there was obtained 115.6 g of 6-chloro-2-phenyl-4-quinolinol, mp greater than 350°.

Sources & evidence

ORD record: ord-30b91eab70b5468b90cfb580f15718d5
Source dataset: uspto-grants-1985_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04560692

Reaction notes

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