HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178465686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 4'-Hydroxyacetophenone | HCID 7469 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178465686 | HCID 178465686 | 99.9% |
Reaction Steps
A solution was prepared by adding 13.6 g (0.1 mol) of 4-hydroxyacetophenone, 7.6 g (0.11 mol) of hydroxylamine hydrochloride, and 10 g of water to 40 mL of ethanol. To the solution was added 5.0 g of 30% ammonium hydroxide which was then heated at reflux for 2 h. The ethanol was removed on a rotary evaporator to yield a yellow oil. An extractive work-up afforded 15.1 g (99%) of 4-hydroxyacetophenone oxime.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04560789 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-d3f2ed5d0acc408f8b10dd27773cbdf3 |
| Source note | uspto-grants-1985_12 |