HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 20252401, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 20252423 | HCID 20252423 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20252401 | HCID 20252401 | — |
Reaction Steps
To a solution of ethyl 4-[4-(2-nitro-4-chlorophenoxy)phenoxy]-3-oxopentanoate (600 mg) in absolute ethanol (10 ml) is added at 0°, NaBH4 (300 mg). After addition is complete, the reaction mixture is stirred for about 20 minutes. Then the solution is taken up in CH2Cl2, washed with brine, dried and evaporated to give ethyl 4-[4-(2-nitro-4-chlorophenoxy)phenoxy]-3-hydroxypentanoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04561882 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-22ac34d6e0fa4738ad4e344272734ed6 |
| Source note | uspto-grants-1985_12 |