HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 2,4-Di(propan-2-yl)spiro[5.5]undeca-1,4,8-trien-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Propofol | HCID 4943 | — |
| Reactant | 1,3-Butadiene | HCID 7845 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 2,4-Di(propan-2-yl)spiro[5.5]undeca-1,4,8-trien-3-one | HCID 13574726 | — |
Reaction Steps
Following the same general procedure as in Example I, 50 mmols of 2,6-diisopropylphenol were reacted with 75 mmols of paraformaldehyde, 75 mmols of aqueous dimethylamine, and 210 mmols of 1,3-butadiene in 100 g of isopropyl alcohol at 190°-200° C. for five hours. The process resulted in the formation of 2,4-diisopropylspiro[5.5]undeca-1,4,8-trien-3-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04562293 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-cd9c511510a0404c99b5009e26ffaae6 |
| Source note | uspto-grants-1985_12 |