HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Butadiene → HCID 13531454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Butadiene | HCID 7845 | — |
| Reactant | 2-tert-Butyl-4-[(dimethylamino)methyl]-6-methylphenol | HCID 231476 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13531454 | HCID 13531454 | — |
Reaction Steps
Following the same general procedure as in Example I, 40 mmols of N,N-dimethyl-4-aminomethyl-2-methyl-6-t-butylphenol were reacted with 80 mmols of 1,3-butadiene in 81 g of toluene at about 207° C. for 10 hours. The uncorrected isolated yield of 2-methyl-4-t-butylspiro[5.5]undeca-1,4,8-trien-3-one was 83%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04562294 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-f15421c109c94208986dfdbb72178fa2 |
| Source note | uspto-grants-1985_12 |