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HRID638666

反应详情

EQUATION

反应方程式

HRID 638666 的结构方程式

REACTANTS

反应物

2
结构：C=CC=C
HCID7845

1,3-Butadiene

C4H6

结构：Cc1cc(CN(C)C)cc(C)c1O
HCID39355

Phenol, 4-[(dimethylamino)methyl]-2,6-dimethyl-

C11H17NO

PRODUCTS

生成物

1
结构：CC1=CC2(C=C(C)C1=O)CC=CCC2
HCID13531455

未命名化合物

收率 78%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

Following the same general procedure as in Example I, 5 mmols of N,N-dimethyl-4-aminomethyl-2,6-dimethylphenol were reacted with 20 mmols of 1,3-butadiene in 40 g of toluene at 189°-205° C. for six hours. GC analysis showed a 78% yield of 2,4-dimethylspiro[5.5]undeca-1,4,8-trien-3-one.