HuagongsheHuagongshe Chemistry Print Report · For research reference only
NSC697569 → HCID 11817172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | NSC697569 | HCID 394240 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 11817172 | HCID 11817172 | 40% |
Reaction Steps
7-methoxy imidazo[2,1-b]-benzthiazole-2-methanol was prepared according to the procedure outlined in Example 1, (Step 2). Starting from ethyl 7-methoxyimidazo[2,1-b]-benzthiazole-2-carboxylate (12.5 g, 43.5 mmol) and LiAlH4 solution (43.5 ml, 0.5 M solution in THF), 4.0 g (40% yield) of the alcohol derivative was isolated as a brown solid. (M+H) 235.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691842B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-7b3e2bb4fc114058bc4d0b63f424c403 |
| Source note | uspto-grants-2010_04 |