HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11172083, compound → HCID 11229736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11172083 | HCID 11172083 | — |
| Solvent | Manganese dioxide | HCID 14801 | — |
| Solvent | dichloromethane N,N-dimethylformamide | HCID 22350042 | — |
| Product | HCID 11229736 | HCID 11229736 | — |
Reaction Steps
2-Formyl-7-fluoro-imidazo[2,1-b]-benzthiazole was prepared according to the procedure outlined in Example 1, (Step 3). Starting from 7-fluoro-imidazo[2,1-b]-benzthiazole-2-methanol (1.5 g 6.7 mmol) in methylene chloride/DMF (300 mL: 50 mL) and active MnO2 (12 g, excess), 1.1 g (78% Yield) of the aldehyde derivative was isolated as brown solid. (M+H) 221.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691842B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-c914c2ca5c454c06bb446117406e9d63 |
| Source note | uspto-grants-2010_04 |