HRID638947

反应详情

EQUATION

反应方程式

HRID 638947 的结构方程式

PROCEDURE

实验过程

4-Bromo-1-methylthio-2-trifluoromethoxybenzene was prepared from 4-bromo-2-trifluoromethoxybenzenethiol and methyl iodide by following Method C. The reaction was conducted at room temperature overnight. The crude residue was chromatographed in 20% EtOAc/Hexanes to afford 4-bromo-1-methylthio-2-trifluoromethoxybenzene (85% yield).

WORKUP

后处理

  1. customThe crude residue was chromatographed in 20% EtOAc/Hexanes