HRID639061

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID21004

Dichloromethyl methyl ether

C2H4Cl2O

HCID12464545

6-Fluoro-2,3-dihydro-1,4-benzodioxine

C8H7FO2

PRODUCTS

生成物

HCID14644883

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID24193

Titanium tetrachloride

Cl4Ti

PROCEDURE

实验过程

7-Fluoro-2,3-dihydrobenzo[1,4]dioxine-6-carboxaldehyde was prepared from 6-fluoro-2,3-dihydrobenzo[1,4]dioxine [V. Daukas et al Chemija, 1999, 10 (1), 59] by reaction of dichloromethyl methyl ether and titanium tetrachloride: LC-MS (ES) m/e 155 (M+H)+.