HRID639124

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID20443148

1,4-Dioxane hydrochloride

C4H9ClO2

$结构：CC(C)(C)OC(=O)N1C/C(=N\O)[C@H](CNC(=O)OCc2ccccc2)C1$

HCID87503005

未命名化合物

PRODUCTS

生成物

$结构：Cl.O=C(NC[C@@H]1CNC/C1=N\O)OCc1ccccc1$

HCID178479734

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Dissolve 1,1-dimethylethyl(3Z,4R)-3-(hydroxyimino)-4-[({[(phenylmethyl)oxy]carbonyl}amino)methyl]-1-pyrrolidinecarboxylate (0.90 g, 2.53 mmol) in methylene chloride (10 mL). Add HCl/dioxane (excess) and stir at ambient temperature for 3 hours. Concentrate solution under reduced pressure. (0.66 g, quant). LCMS: m/z 254.4 (MH+).