HRID639434

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6452000

(1,1'-Biphenyl)-3,4-diamine

C12H12N2

结构：CN([C@H]1CC[C@H](C(=O)O)CC1)S(=O)(=O)C(C)(C)C

HCID178484816

未命名化合物

PRODUCTS

生成物

结构：CN([C@H]1CC[C@H](c2nc3ccc(-c4ccccc4)cc3[nH]2)CC1)S(=O)(=O)C(C)(C)C

HCID178484789

未命名化合物

PROCEDURE

实验过程

Trans-4-(N-methyl-tert-butylsulfonylamino)cyclohexanecarboxylic acid and 4-phenyl-1,2-phenylenediamine were allowed to undergo ring closure condensation under the same conditions as described in Example 1-3), followed by separatory purification on a collective thin-layer chromatograph (chloroform:methanol=10:1) to give the title compound.

WORKUP

后处理

customring closure condensation under the same conditions
customfollowed by separatory purification on a collective thin-layer chromatograph (chloroform:methanol=10:1)