3-Pyridinecarbonyl chloride, hydrochloride (1:1) → N,4-dimethyl-5-pyridin-3-yl-4H-1,2,4-triazol-3-amine

HRID 639786Notes

Reaction equation

HRID 639786 reaction equation
[CH3:1][NH:2][C:3]1[N:7]([CH3:8])[C:6]([C:9]2[CH:14]=[CH:13]N=C[CH:10]=2)=[N:5][N:4]=1.Cl.C(Cl)(=O)C1C=CC=[N:19][CH:18]=1>>[CH3:1][NH:2][C:3]1[N:7]([CH3:8])[C:6]([C:9]2[CH:10]=[N:19][CH:18]=[CH:13][CH:14]=2)=[N:5][N:4]=1

Participants

3

Reactant 2

HCID 884383-Pyridinecarbonyl chloride, hydrochloride (1:1)HCID 57837980Methyl-(4-methyl-5-pyridin-4-yl4H-[1,2,4]triazol-3-yl)-amine

Product 1

HCID 57837974N,4-dimethyl-5-pyridin-3-yl-4H-1,2,4-triazol-3-amine

Procedure

The title compound is prepared according to the procedure for methyl-(4-methyl-5-pyridin-4-yl-4H-[1,2,4]triazol-3-yl)-amine (example 16a) from nicotinoyl chloride hydrochloride.

Sources & evidence

ORD record
ord-cfa91c54812745aeaf9ba349301c9100
Source dataset
uspto-grants-2010_04
Patent number
US07691892B2

Reaction notes

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