HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → [(3-Bromo-3-buten-1-yl)oxy](1,1-dimethylethyl)diphenylsilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | tert-Butyldiphenylchlorosilane | HCID 94078 | — |
| Reactant | 3-Bromo-3-buten-1-ol | HCID 533975 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | [(3-Bromo-3-buten-1-yl)oxy](1,1-dimethylethyl)diphenylsilane | HCID 11784074 | — |
Reaction Steps
The title compound was prepared in 8.7 g yield as a colourless oil, following an analogous procedure to that reported in WO2005058884, starting from 3-bromo-3-buten-1-ol (4 g), chloro(1,1-dimethylethyl)diphenylsilane (8.27 ml), imidazole (2.34 g) and N,N-dimethyl-4-pyridineamine (0.025 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691893B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-c804fc82019244ec96cd507ab87da29e |
| Source note | uspto-grants-2010_04 |