HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68541822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 24802846 | HCID 24802846 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68541822 | HCID 68541822 | 195.6% |
Reaction Steps
To a solution of (1R,6S)-6-(3,4-dichlorophenyl)-3-azabicyclo[4.1.0]heptane (E9a, 40 mg) in DCM was added 1 equivalent of HCl (1M in Et2O), the solvent evaporated in vacuo and the material thus obtained triturated with Et2O to give 45 mg of the title compound as a white slightly hygroscopic solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691893B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-0b80c6ffed8649d6b2ac133c3e95d9f1 |
| Source note | uspto-grants-2010_04 |