HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68551076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 24802845 | HCID 24802845 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68551076 | HCID 68551076 | 195.6% |
Reaction Steps
To a solution of (1S,6R)-6-(3,4-dichlorophenyl)-3-azabicyclo[4.1.0]heptane (E10a, 40 mg) in DCM was added 1 equivalent of HCl (1M in Et2O), the solvent evaporated in vacuo and the material thus obtained triturated with Et2O to give 45 mg of the title compound as a white slightly hygroscopic solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07691893B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-9bb8a8206c2249e286e1d4b033169612 |
| Source note | uspto-grants-2010_04 |