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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 640240Generated: October 26, 2026

(4-(5-Chloro-furan-2-ylmethyl)-phenyl)-methanol → HCID 59255186, compound

https://huagongshe.com/reaction/640240

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(4-(5-Chloro-furan-2-ylmethyl)-phenyl)-methanolHCID 59255370—
CatalystHCID 178418406HCID 178418406—
SolventDichloromethaneHCID 6344—
ProductHCID 59255186HCID 5925518683%

Reaction Steps

To a mixture of (4-(5-chloro-furan-2-ylmethyl)-phenyl)-methanol (650 mg, 2.9 mmol) described in Manufacturing Example 62-1-3 and dichloromethane (20 mL) was added manganese dioxide (6.5 g, 75 mmol) at room temperature, which was stirred overnight at room temperature. The reaction mixture was filtered through a Celite pad. The filtrate was evaporated under a reduced pressure to obtain the title compound (530 mg, 83%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07691882B2
Source datasetuspto-grants-2010_04
ORD IDord-8ac777820b7e4a6fb8c7c5f5f6181e61
Source noteuspto-grants-2010_04