HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tin dichloride dihydrate → HCID 59256807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tin dichloride dihydrate | HCID 43835034 | — |
| Reactant | HCID 59256662 | HCID 59256662 | — |
| Product | HCID 59256807 | HCID 59256807 | 93% |
Reaction Steps
Reduction of 4,6-dichloro-N-cyclopropyl-3-hydroxy-2-nitrobenzamide with tin (II) chloride hydrate using the conditions as described in Step B yielded 2-amino-4,6-dichloro-N-cyclopropyl-3-hydroxybenzamide (93%).—1H NMR (CD3OD): δ 6.67 (s, 1H), 2.86 (m, 1H), 0.79 (m, 2H), 0.62 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07692011B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-0f5bc633ea1e480488861d85e2f76556 |
| Source note | uspto-grants-2010_04 |