Cyclopropanesulfonyl chloride → HCID 117777809, compound

Participants

Reaction Steps

The compound was prepared from the compound of Example 87 using the procedures of Example 88 and cyclopropane sulfonyl chloride. 1H-NMR (300 MHz, DMSO-d6): δ 10.2 (s, 1H), 8.71 (s, 1H), 8.2 (s, 1H), 7.99 (m, 1H), 7.95 (s, 1H), 7.68-7.59 (m, 3H), 7.44-7.41 (m, 4H), 6.31 (m, 2H), 3.95 (s, 3H), 2.95 (m, 1H), 1.0 (m, 4H); LC-MS (ESI): Calculated mass: 458.54; Observed mass: 459.2 [M+H]+ (rt: 1.29 min).

Provenance & Evidence